1,2-二溴-3,4,5,6-四氢甲基苯合成路线 (共 8 条)
反应条件
bromine; iodine in dichloromethane 3 h;
参考文献
Wenderski, Todd; Light, Kenneth M.; Ogrin, Doug; Bott, Simon G.; Harlan, C. Jeff
Tetrahedron Letters, 2004 , vol. 45, # 37 p. 6851 - 6853
反应条件
benzyltrimethylammonium bromide dibromide; zinc(II) chloride in acetic acid 2 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 2 p. 439 - 443
参考文献
Journal of the American Chemical Society, , vol. 55, p. 1676,1681
参考文献
Journal of the American Chemical Society, , vol. 55, p. 1676,1681
参考文献
Smith; Moyle
Journal of the American Chemical Society, 1933 , vol. 55, p. 1676,1681
反应条件
1: 2-bromo-1,3,5-triisopropylbenzene With magnesium; ethylene dibromide in tetrahydrofuran T=60°C; 0.25 h; 2: 1,2-Dibromo-3,4,5,6-tetramethylbenzene in tetrahydrofuran T=60°C; 1.5 h; 3: chlorodi-tert-butylphosphine With copper(l) iodide in tetrahydrofuran T=75°C; 40 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 22 p. 8146 - 8149
参考文献
Kreher, Richard P.; Hildebrand, Thomas
Angewandte Chemie, 1987 , vol. 99, # 12 p. 1325 - 1327
反应条件
bromine in tetrachloromethane
24 h; HeatingIrradiation;
参考文献
Lin, Lon-Tang Wilson; Hart, Harold
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1027 - 1030