溴(2-甲氧基-1-萘基)镁合成路线 （共 6 条）
反应条件
1: THF 2: aqueous KOH View Scheme
参考文献
Broquet-Borgel
Annales de Chimie (Cachan, France), 1958 , vol. <13> 3, p. 204,248
反应条件
bis(imidazol-1-yl) sulphoxide in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Bell, Kevin H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1957 - 1960
反应条件
in tetrahydrofuran; benzene
18 h; Heating;
参考文献
Hattori; Sakamoto; Hayashizaka; Miyano
Synthesis, 1994 , # 2 p. 199 - 202
反应条件
1: 92 percent / Cs2CO3; Pd(OAc)2; PPh3 / o-xylene / 2.5 h / Heating
View Scheme
参考文献
Terao, Yoshito; Wakui, Hiroyuki; Nomoto, Michiyo; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5236 - 5243
反应条件
diethyl ether
Erhitzen des Reaktionsprodukts mit Schwefel auf 250grad bis 275grad;
参考文献
Berson; Greenbaum
Journal of the American Chemical Society, 1958 , vol. 80, p. 653,655
反应条件
1.1: tetrahydrofuran; diethyl ether / -78 - 0 °C / Inert atmosphere
2.1: lithium hexamethyldisilazane / tetrahydrofuran; diethyl ether / 0 - 20 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
View Scheme
参考文献
Han, Zhengxu S.; Meyer, Angelica M.; Xu, Yibo; Zhang, Yongda; Busch, Robert; Shen, Sherry; Grinberg, Nelu; Lu, Bruce Z.; Krishnamurthy, Dhileep; Senanayake, Chris H.
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5480 - 5484
