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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
36332-93-1
合成路线
（共 13 条）
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反应条件
36332-93-1
反应条件
sulfuric acid; acetic acid
参考文献
Kao Corporation
Patent: US5476649 A1, 1995 ;
65301-92-0
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反应条件
36332-93-1
反应条件
potassium hydroxide in ethanol T=20°C; Hydrolysis; 17 h;
参考文献
Cundy, Darren J.; Gurr, Paul A.
Organic Preparations and Procedures International, 2000 , vol. 32, # 5 p. 461 - 468
106-02-5
环十五内酯
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反应条件
36332-93-1
反应条件
1: 99 percent / p-TosH*H2O / 24 h / Heating 2: oxalyl chloride; DMSO; triethylamine / CH2Cl2 / 0.33 h / -10 °C 3: 28 percent / nBuLi / tetrahydrofuran / 0 °C 4: 99 percent / H2 / 10 percent Pd/C / ethyl acetate / 26 h 5: 88 percent / aq. KOH / ethanol / 17 h / 20 °C View Scheme
参考文献
Cundy, Darren J.; Gurr, Paul A.
Organic Preparations and Procedures International, 2000 , vol. 32, # 5 p. 461 - 468
76529-42-5
15-羟基十五烷酸甲酯
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反应条件
36332-93-1
反应条件
1: oxalyl chloride; DMSO; triethylamine / CH2Cl2 / 0.33 h / -10 °C 2: 28 percent / nBuLi / tetrahydrofuran / 0 °C 3: 99 percent / H2 / 10 percent Pd/C / ethyl acetate / 26 h 4: 88 percent / aq. KOH / ethanol / 17 h / 20 °C View Scheme
参考文献
Cundy, Darren J.; Gurr, Paul A.
Organic Preparations and Procedures International, 2000 , vol. 32, # 5 p. 461 - 468
589-35-5
3-甲基-1-戊醇
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反应条件
36332-93-1
反应条件
1: 78 percent / aq. H2SO4; HBr / 72 h / Heating 2: 74 percent / (n-Bu)4NI / toluene / 240 h / Heating 3: 28 percent / nBuLi / tetrahydrofuran / 0 °C 4: 99 percent / H2 / 10 percent Pd/C / ethyl acetate / 26 h 5: 88 percent / aq. KOH / ethanol / 17 h / 20 °C View Scheme
参考文献
Cundy, Darren J.; Gurr, Paul A.
Organic Preparations and Procedures International, 2000 , vol. 32, # 5 p. 461 - 468
1931-69-7
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反应条件
36332-93-1
反应条件
1: 28 percent / nBuLi / tetrahydrofuran / 0 °C 2: 99 percent / H2 / 10 percent Pd/C / ethyl acetate / 26 h 3: 88 percent / aq. KOH / ethanol / 17 h / 20 °C View Scheme
参考文献
Cundy, Darren J.; Gurr, Paul A.
Organic Preparations and Procedures International, 2000 , vol. 32, # 5 p. 461 - 468
51116-73-5
1-溴-3-甲基戊烷
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反应条件
36332-93-1
反应条件
1: 74 percent / (n-Bu)4NI / toluene / 240 h / Heating 2: 28 percent / nBuLi / tetrahydrofuran / 0 °C 3: 99 percent / H2 / 10 percent Pd/C / ethyl acetate / 26 h 4: 88 percent / aq. KOH / ethanol / 17 h / 20 °C View Scheme
参考文献
Cundy, Darren J.; Gurr, Paul A.
Organic Preparations and Procedures International, 2000 , vol. 32, # 5 p. 461 - 468
72279-54-0
→
反应条件
36332-93-1
反应条件
1: 28 percent / nBuLi / tetrahydrofuran / 0 °C 2: 99 percent / H2 / 10 percent Pd/C / ethyl acetate / 26 h 3: 88 percent / aq. KOH / ethanol / 17 h / 20 °C View Scheme
参考文献
Cundy, Darren J.; Gurr, Paul A.
Organic Preparations and Procedures International, 2000 , vol. 32, # 5 p. 461 - 468
316826-17-2
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反应条件
36332-93-1
反应条件
1: 97 percent / m-chloroperbenzoic acid; NaHCO3 / CH2Cl2 / 24 h 2: 30 percent / NaHMDS / tetrahydrofuran / -78 °C 3: 99 percent / H2 / 10 percent Pd/C / ethyl acetate / 26 h 4: 88 percent / aq. KOH / ethanol / 17 h / 20 °C View Scheme
参考文献
Cundy, Darren J.; Gurr, Paul A.
Organic Preparations and Procedures International, 2000 , vol. 32, # 5 p. 461 - 468
316826-18-3
→
反应条件
36332-93-1
反应条件
1: 97 percent / magnesium monoperphthalate hexahydrate / ethanol / 20 °C 2: 30 percent / NaHMDS / tetrahydrofuran; 1,2-dimethoxy-ethane / 20 h / -65 - 20 °C 3: 99 percent / H2 / 10 percent Pd/C / ethyl acetate / 26 h 4: 88 percent / aq. KOH / ethanol / 17 h / 20 °C View Scheme
参考文献
Cundy, Darren J.; Gurr, Paul A.
Organic Preparations and Procedures International, 2000 , vol. 32, # 5 p. 461 - 468
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