3-氯-2,6-二甲氧基苯甲酸合成路线 （共 7 条）
反应条件
thionyl chloride in chloroform T=50°C; 0.5 h;
参考文献
Florvall, Lennart; Oegren, Sven-Ove
Journal of Medicinal Chemistry, 1982 , vol. 25, # 11 p. 1280 - 1286
参考文献
Cartwright et al.
Journal of the Chemical Society, 1952 , p. 3499,3502
反应条件
aluminium trichloride
参考文献
Cartwright et al.
Journal of the Chemical Society, 1952 , p. 3499,3502
反应条件
1: AlCl3 2: 260 °C View Scheme
参考文献
Cartwright et al.
Journal of the Chemical Society, 1952 , p. 3499,3502
反应条件
bromine; sodium acetate in acetic acid
Ambient temperature;
参考文献
Florvall, Lennart; Oegren, Sven-Ove
Journal of Medicinal Chemistry, 1982 , vol. 25, # 11 p. 1280 - 1286
反应条件
1: 17 percent / Br2, AcONa / acetic acid / Ambient temperature
2: SOCl2 / 1 h / Heating
3: butan-2-one / 0.5 h
View Scheme
参考文献
Florvall, Lennart; Oegren, Sven-Ove
Journal of Medicinal Chemistry, 1982 , vol. 25, # 11 p. 1280 - 1286
反应条件
1: 17 percent / Br2, AcONa / acetic acid / Ambient temperature
2: SOCl2 / 1 h / Heating
View Scheme
参考文献
Florvall, Lennart; Oegren, Sven-Ove
Journal of Medicinal Chemistry, 1982 , vol. 25, # 11 p. 1280 - 1286
