in further solvent(s) under vac.; in NMR tube charged In complex and C6D5Cl at -78°C; the tube was maintained at 23°C for 10 ds; not isolated; monitored by NMR;
参考文献
Delpech, Fabien; Guzei, Ilia A.; Jordan, Richard F.
Organometallics, 2002 , vol. 21, # 6 p. 1167 - 1176
in deuterated toluene warming to room temp. in toluene-d8/bromobenzene-d5;
参考文献
Metcalfe, Robert A.; Kreller, David I.; Tian, Jun; Kim, Hoon; Taylor, Nicholas J.; Corrigan, John F.; Collins, Scott
Organometallics, 2002 , vol. 21, # 8 p. 1719 - 1726
in benzene-d6 under Ar; in NMR tube; Al complex and B(C6F5)3 (molar ratio 2:1) dissolved in benzene-d6; stirred at room temp. for 12 h; not isolated; monitored by NMR spectra;
参考文献
Amo, Virginia; Andres, Roman; De Jesus, Ernesto; De La Mata, F. Javier; Flores, Juan C.; Gomez, Rafael; Gomez-Sal, M. Pilar; Turner, John F. C.
Organometallics, 2005 , vol. 24, # 10 p. 2331 - 2338
in benzene-d6 under Ar; in NMR tube; Ti complex and B(C6F5)3 (molar ratio 2:1) dissolved in benzene-d6 at room temp.; shaken; maintained at room temp. (296 K)for 22 h; not isolated; monitored by (1)H NMR spectra; mixt. of Ti-CH2C6F5 and Ti-Me complexes (3:97), BMe(C6F5)2 and BMe2(C6F5) obtained;
参考文献
Amo, Virginia; Andres, Roman; De Jesus, Ernesto; De La Mata, F. Javier; Flores, Juan C.; Gomez, Rafael; Gomez-Sal, M. Pilar; Turner, John F. C.
Organometallics, 2005 , vol. 24, # 10 p. 2331 - 2338
in benzene-d6 (Ar, Schlenk) a NMR-tube was charged with complex and B(C6F5)3, dissolved in C6D6 at room temp., 5 min to 6 days; detected by NMR spectra;
