2-[2-[2-(2-苯氧乙氧基]乙氧基]乙氧基]乙醇合成路线 （共 16 条）
参考文献
Kimura, Masaru; Kajita, Kazushige; Onoda, Naoyuki; Morosawa, Shiro
Journal of Organic Chemistry, 1990 , vol. 55, # 16 p. 4887 - 4892
反应条件
phenolated sodium T=200°C;
参考文献
Miller et al.
Journal of the Chemical Society, 1950 , p. 3623,3628
反应条件
potassium hydroxide in butan-1-ol 16 h; Heating; Yield given;
参考文献
Loehr, Hans-Gerd; Voegtle, Fritz
Chemische Berichte, 1985 , vol. 118, # 3 p. 914 - 921
反应条件
1: 72 percent / pyridine / CH2Cl2 / 13 h / Ambient temperature
2: 90 percent / H2 / 10percent Pd/C / ethanol / 8 h / 2585.7 Torr
3: 48percent HBF4, NaNO2 / H2O / 0.17 h / 0 °C
4: NaOAc / 1,1,2-trichloro-1,2,2-trifluoro-ethane / 24 h
View Scheme
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
反应条件
pyridine in dichloromethane
13 h; Ambient temperature;
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
反应条件
1: 72 percent / pyridine / CH2Cl2 / 13 h / Ambient temperature
2: 90 percent / H2 / 10percent Pd/C / ethanol / 8 h / 2585.7 Torr
View Scheme
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
