4-(4-甲基苯基)苯甲醛合成路线 （共 31 条）
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy in tetrahydrofuran T=63°C; 0.75 h; Yields of byproduct given;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy in tetrahydrofuran T=63°C; 4.5 h; Yields of byproduct given;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy in tetrahydrofuran T=63°C; 2.5 h; Yields of byproduct given;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy in tetrahydrofuran T=63°C; 1.5 h; Yields of byproduct given;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848
反应条件
1: triphenylphosphine; AcOK / PdCl2(PPh3)2 / toluene / Heating 2: Na2CO3; Bu4NHSO4 / Pd(PPh3)4 / H2O; toluene / Heating View Scheme
参考文献
Synthetic Communications, , vol. 37, # 5 p. 667 - 674
反应条件
potassium carbonate in ethanol; water T=50°C; Suzuki coupling; 24 h;
参考文献
European Journal of Organic Chemistry, , # 13 p. 2635 - 2642
反应条件
hydrogenchloride in diethyl ether Yield given;
参考文献
Tetrahedron, , vol. 46, # 23 p. 7813 - 7822
反应条件
1: sodium sulfate / tetrahydrofuran / 24 h / 20 °C / |Schlenk technique; |Inert atmosphere 2: palladium diacetate; dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium carbonate / neat (no solvent) / 24 h / 110 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 18 p. 3553 - 3557
反应条件
polymethylhydrosiloxane; FeCl3*6H2O in 1,2-dichloro-ethane T=120°C; 1 h; Microwave irradiation;
参考文献
Dal Zotto, Christophe; Virieux, David; Campagne, Jean-Marc
Synlett, 2009 , # 2 p. 276 - 278
