2-氟-1,3,5-三硝基-苯合成路线 （共 22 条）
反应条件
in dimethylsulfoxide-d6 Ambient temperaturemonitored by 1H-NMR; further solvent and temperature; MechanismProduct distribution;
参考文献
Manderville, Richard A.; Dust, Julian M.; Buncel, Erwin
Journal of Physical Organic Chemistry, 1996 , vol. 9, # 8 p. 515 - 528
反应条件
in acetonitrile-D3 T=-40°C; monitored by 1H-NMR; different quantity of the phenolate; further solvent and temperature; MechanismProduct distribution;
参考文献
Manderville, Richard A.; Dust, Julian M.; Buncel, Erwin
Journal of Physical Organic Chemistry, 1996 , vol. 9, # 8 p. 515 - 528
反应条件
lithium bis(trimethylstannyl)cuprate in tetrahydrofuran; hexane
further reagents (Me3SnLi);
参考文献
Artamkina, G. A.; Egorov, M. P.; Beletskaya, I. P.; Reutov, O. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 1649 - 1659
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 8 p. 1809 - 1820
参考文献
Sharnin,G.P. et al.
Zhurnal Organicheskoi Khimii, 1968 , vol. 4, # 5 p. 858 - 860,834 - 836
反应条件
in dimethylsulfoxide-d6
Ambient temperaturemonitored by 1H-NMR; further solvent and temperature; MechanismProduct distribution;
参考文献
Manderville, Richard A.; Dust, Julian M.; Buncel, Erwin
Journal of Physical Organic Chemistry, 1996 , vol. 9, # 8 p. 515 - 528
反应条件
potassium trimethylstannate
THF; Multistep reaction;
参考文献
Artamkina, G. A.; Egorov, M. P.; Beletskaya, I. P.; Reutov, O. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 1649 - 1659
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 8 p. 1809 - 1820
反应条件
in tetrahydrofuran
vac., 50°C, 36 h; NMR and UV spectroscopy;
参考文献
Artamkina, G. A.; Egorov, M. P.; Kharitonov, V. G.; Beletskaya, I. P.; Reutov, O. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 2 p. 432
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 2 p. 476 - 477
反应条件
in tetrahydrofuran
48 h; other solvent (benzene); other reaction time (8d); Product distributionMechanism;
参考文献
Artamkina, G. A.; Egorov, M. P.; Beletskaya, I. P.; Reutov, O. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 1649 - 1659
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 8 p. 1809 - 1820
反应条件
tetrabutylammonium trifluoromethanesulphonate in tetrachloromethane
T=25°C; Substitution; Kinetics;
参考文献
Forlani, Luciano; Boga, Carla; Forconi, Marcello
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 7 p. 1455 - 1458
反应条件
in tetrachloromethane
T=25°C; Substitution; Kinetics;
参考文献
Forlani, Luciano; Boga, Carla; Forconi, Marcello
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 7 p. 1455 - 1458
