4-氟-1-碘-2-硝基苯合成路线 （共 6 条）
反应条件
sulfuric acid Diazotization.Umsetzen der Diazoniumsalz-Loesung mit Kaliumjodid-Loesung;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 36, p. 375,376
Chem. Zentralbl., , vol. 98, # I p. 886
Bl. Acad. Belg., vol. <5> 12, p. 827
反应条件
sulfuric acid; potassium iodide; sodium nitrite 1) water, 0-5 deg C, 4 h; 2) 80-85 deg C, 1.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 52, # 7 p. 1811 - 1833
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=90 - 100°C; 3 h; Yield given;
参考文献
Protiva, Miroslav; Jilek, Jiri; Rajsner, Miroslav; Sindelar, Karel; Bartl, Vaclav; et al.
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 7 p. 1811 - 1833
反应条件
1) 90-95 deg C, 2 h; 2) room temp., overnight; Yields of byproduct given;
参考文献
Protiva, Miroslav; Jilek, Jiri; Rajsner, Miroslav; Sindelar, Karel; Bartl, Vaclav; et al.
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 7 p. 1811 - 1833
反应条件
1: hexamethylphosphoric acid triamide / 3 h / 90 - 100 °C 2: 90 percent / H2SO4 / H2O / 6 h / 160 - 170 °C View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 52, # 7 p. 1811 - 1833
反应条件
copper(l) iodide; 1,10-phenanthroline; Na2S*9H2O in acetic acid T=100°C; 12 h; Sealed tube;
参考文献
Liu, Jidan; Gui, Qingwen; Yang, Zhiyong; Tan, Ze; Guo, Ruqing; Shi, Ji-Cheng
Synthesis (Germany), 2013 , vol. 45, # 7 art. no. SS-2012-F0968-OP, p. 943 - 951
