lithium diisopropyl amide in tetrahydrofuran T=-70°C;
参考文献
Jeff Thrasher; Hembre, Erik J.; Gardinier, Kevin M.; Savin, Kenneth A.; Hong, Jian Eric; Jungheim, Louis N.
Heterocycles, 2006 , vol. 67, # 2 p. 543 - 547
diisobutylaluminium hydride in dichloromethane T=-78°C; 3 h;
参考文献
New, James S.; Yevich, Joseph P.; Temple, Davis L.; New, Kimberly B.; Gross, Sharon M.; et al.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 3 p. 618 - 624
1: With 3,4,5,6-tetrahydro-1(2H)-pyrimidinone; n-butyllithium; diisopropylamine in tetrahydrofuran T=-95 - -40°C; 5.5 h; 2: With hydrogenchloride in tetrahydrofuran; water; N,N-dimethyl-formamide 0.0833333 h; 3: With ammonium hydroxide in tetrahydrofuran; water; N,N-dimethyl-formamide pH=7.5;
