7-[[(2E)-3-(4,5-二氢-5,5-二甲基-4-氧代-2-呋喃基)-2-丁烯-1-基]氧基]-2H-1-苯并吡喃-2-酮合成路线 （共 59 条）
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene
参考文献
Chen, Kau-Ming; Semple, J. Edward; Joullie, Madeleine M.
Journal of Organic Chemistry, 1985 , vol. 50, # 21 p. 3997 - 4005
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene T=25°C; 1.8 h;
参考文献
Saimoto, Hiroyuki; Hiyama, Tamejiro; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 10 p. 3078 - 3087
反应条件
1: 93.2 percent / K2CO3, KI / dimethylformamide; benzene / 3 h / 85 °C 2: 91.7 percent / acetic acid / H2O / 0.5 h / Heating 3: 75 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 9 h / Heating View Scheme
参考文献
Jackson, Richard F. W.; Raphael, Ralph A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 535 - 539
反应条件
methanesulfonyl chloride; triethylamine in tetrahydrofuran Stork-Kraus dehydration;
参考文献
Carotti, Angelo; Carrieri, Antonio; Chimichi, Stefano; Boccalini, Marco; Cosimelli, Barbara; Gnerre, Carmela; Carotti, Andrea; Carrupt, Pierre-Alain; Testa, Bernard
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 24 p. 3551 - 3555
反应条件
potassium carbonate; lithium iodide; 18-crown-6 ether in acetone 16 h; Heating;
参考文献
Sakai, Takashi; Ito, Hiroshi; Yamawaki, Akitoshi; Takeda, Akira
Tetrahedron Letters, 1984 , vol. 25, # 28 p. 2987 - 2988
反应条件
acetic acid T=0°C; 4 h;
参考文献
Baraldi; Barco; Benetti; et al.
Tetrahedron Letters, 1985 , vol. 26, # 43 p. 5319 - 5322
反应条件
1: 1.) BuLi / 1.) THF, hexane, -78 deg C, 3 h, 2.) THF, hexane, -78 deg C, 3 h 2: pyridine / CH2Cl2 / 3 h / 20 °C 3: AgClO4 / benzene / 10 h / 80 °C 4: 99 percent / DDQ / benzene / 1.8 h / 25 °C View Scheme
参考文献
Inoue, Y.; Ohuchi, K.; Imaizumi, S.; Hagiwara, H.; Uda, H.
Synthetic Communications, 1990 , vol. 20, # 19 p. 3063 - 3068
反应条件
1: pyridine / CH2Cl2 / 3 h / 20 °C 2: AgClO4 / benzene / 10 h / 80 °C 3: 99 percent / DDQ / benzene / 1.8 h / 25 °C View Scheme
参考文献
Inoue, Y.; Ohuchi, K.; Imaizumi, S.; Hagiwara, H.; Uda, H.
Synthetic Communications, 1990 , vol. 20, # 19 p. 3063 - 3068
反应条件
potassium carbonate; lithium bromide in acetone Heating;
参考文献
Jackson, Richard F. W.; Raphael, Ralph A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 3 p. 535 - 539
反应条件
1: SeO2 3: pyridine / Ambient temperature 4: 61 percent / AgClO4 / benzene / Heating 5: dichlorodicyano-p-benzoquinone / benzene / Ambient temperature View Scheme
参考文献
Inoue, Y.; Ohuchi, K.; Imaizumi, S.; Hagiwara, H.; Uda, H.
Synthetic Communications, 1990 , vol. 20, # 19 p. 3063 - 3068
