4-溴-3-乙基-9-戊-2-烯-4-炔基-2,8-二氧杂双环[5.2.1]癸烷-6-醇合成路线 （共 2 条）
反应条件
1: diazomethyl-trimethyl-silane With lithium diisopropyl amide in tetrahydrofuran; diethyl ether T=-78°C; Inert atmosphere; 2: C14H21BrO4 in tetrahydrofuran; diethyl ether T=-78 - 0°C; Inert atmosphere;
参考文献
Kim, Byungsook; Lee, Miseon; Mi, Jung Kim; Lee, Hyunjoo; Kim, Sanghee; Kim, Deukjoon; Koh, Minseob; Seung, Bum Park; Kye, Jung Shin
Journal of the American Chemical Society, 2008 , vol. 130, # 49 p. 16807 - 16811
反应条件
phosphate buffer; dihydrogen peroxide; sodium bromide in dimethyl sulfoxide T=20°C; 24 h; bromoperoxidase;
参考文献
Fukuzawa
Tetrahedron Letters, 1990 , vol. 31, # 34 p. 4895 - 4898
