2,4-Dihydroxy-6-(6Alpha,10-dihydroxy-trans-1-undecenyl)benzoicacidμ-lactone合成路线 （共 15 条）
反应条件
1: 87 percent / aq. KOH / ethane-1,2-diol / 3 h / 120 °C 2: 64 percent / Et3N; 2-chloro-1-methylpyridinium iodide / acetonitrile / 5 h / Heating 3: aq. HCl / tetrahydrofuran / 48 h / 40 °C View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 7 p. 874 - 882
反应条件
1: 95 percent / HF*pyridine; pyridine / tetrahydrofuran / 12 h / 20 °C 2: 87 percent / aq. KOH / ethane-1,2-diol / 3 h / 120 °C 3: 64 percent / Et3N; 2-chloro-1-methylpyridinium iodide / acetonitrile / 5 h / Heating 4: aq. HCl / tetrahydrofuran / 48 h / 40 °C View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 7 p. 874 - 882
反应条件
sodium tetrahydroborate
参考文献
Journal of Agricultural and Food Chemistry, , vol. 56, # 11 p. 4032 - 4038
反应条件
water T=40°C; 7 h; lipases from pseudomonas species, other lipases; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 48, # 31 p. 6511 - 6520
反应条件
hydrogen; palladium on activated charcoal T=20°C; P=750.075 Torr;
参考文献
Hellwig, Veronika; Mayer-Bartschmid, Anke; Mueller, Hartwig; Greif, Gisela; Kleymann, Gerald; Zitzmann, Werner; Tichy, Hans-Volker; Stadler, Marc
Journal of Natural Products, 2003 , vol. 66, # 6 p. 829 - 837
