2-溴-4-甲基苯基氨基甲酸叔丁酯合成路线 （共 4 条）
反应条件
in tetrahydrofuran 24 h; Heating;
参考文献
So, Won Youn; Song, Ju-Hyun; Jung, Dai-Il
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5658 - 5661
反应条件
1: 2-iodo-4-methylaniline With sodium hexamethyldisilazane in tetrahydrofuran T=20°C; 0.416667 h; 2: di-tert-butyl dicarbonate in tetrahydrofuran T=20°C; 2 h;
参考文献
Yang, Weibo; Wang, Tao; Yu, Yang; Shi, Shuai; Zhang, Tuo; Hashmi, A. Stephen K.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 8 p. 1523 - 1528
反应条件
trifluoroacetic acid in dichloromethane T=20°C; 16 h;
参考文献
Kessler, Albane; Coleman, Claire M.; Charoenying, Patchanee; O'Shea, Donal F.
Journal of Organic Chemistry, 2004 , vol. 69, # 23 p. 7836 - 7846
反应条件
1: 4-dimethylaminopyridine / tetrahydrofuran / 24 h / Heating 2: 2.4 g / CF3CO2H / CH2Cl2 / 16 h / 20 °C View Scheme
参考文献
Kessler, Albane; Coleman, Claire M.; Charoenying, Patchanee; O'Shea, Donal F.
Journal of Organic Chemistry, 2004 , vol. 69, # 23 p. 7836 - 7846
