2-硝基重氮苯四氟硼酸盐合成路线 （共 41 条）
反应条件
potassium acetate; 18-crown-6 ether 1.5 h; Ambient temperature;
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
反应条件
palladium diacetate in acetonitrile 0.5 h; Ambient temperature;
参考文献
Kikukawa, Kiyoshi; Idemoto, Tohru; Katayama, Atsuhiko; Kono, Kiyoshi; Wada, Fumio; Matsuda, Tsutomu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1511 - 1514
反应条件
iodine; potassium iodide in dimethyl sulfoxide T=15°C;
参考文献
Citterio, Attilio; Arnold, Anna
Synthetic Communications, 1981 , vol. 11, # 8 p. 639 - 642
反应条件
1: With palladium diacetate in 1,4-dioxane T=60°C; Heck reduction-cyclisation reaction; 12 h; 2: With hydrogen; palladium diacetate; carbon in 1,4-dioxane T=50°C; Heck reduction-cyclisation reaction; 24 h;
参考文献
Felpin, Francois-Xavier; Coste, Jerome; Zakri, Cecile; Fouquet, Eric
Chemistry - A European Journal, 2009 , vol. 15, # 29 p. 7238 - 7245
反应条件
sodium nitrite in water T=25 - 29.9°C; Kinetics;
参考文献
Starkey
Journal of the American Chemical Society, 1937 , vol. 59, p. 1479
Organic Syntheses, Col. Vol. II <1943> 225, 226
反应条件
1: With palladium diacetate in 1,4-dioxane T=60°C; Heck reduction-cyclisation reaction; 12 h; 2: With hydrogen; palladium diacetate; carbon in 1,4-dioxane T=50°C; Heck reduction-cyclisation reaction; 24 h;
参考文献
Felpin, Francois-Xavier; Coste, Jerome; Zakri, Cecile; Fouquet, Eric
Chemistry - A European Journal, 2009 , vol. 15, # 29 p. 7238 - 7245
反应条件
1: H2O / 0.17 h / 0 °C 2: 24.20 g / Na / ethanol / 1 h / 20 °C View Scheme
参考文献
Wang, Rui; Chen, Lingxin; Liu, Ping; Wang, Yunqing; Zhang, Qin
Chemistry--A European Journal, 2012 , vol. 18, # 36 p. 11343 - 11349,7
反应条件
1.1: H2O / 0.17 h / 0 °C 2.1: 24.20 g / Na / ethanol / 1 h / 20 °C 3.1: NaSH*H2O; aq. NaOH / 20 °C 3.2: 90 percent / aq. NaOH / 2 h / Heating View Scheme
参考文献
Casar, Zdenko; Leban, Ivan; Marechal, Alenka Majcen-Le; Lorcy, Dominique
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 13 p. 1568 - 1573
参考文献
Yoneda, Norihiko; Fukuhara, Tsuyoshi; Mizokami, Takao; Suzuki, Akira
Chemistry Letters, 1991 , # 3 p. 459 - 460
反应条件
in acetonitrile T=50°C; Arylation; Trifluoromethylthiodediazoniation; 0.5 h;
参考文献
Adams, Dave J.; Goddard, Andrew; Clark, James H.; Macquarrie, Duncan J.
Chemical Communications, 2000 , # 11 p. 987 - 988
