trifluoroacetic acid in dichloromethane
T=20°C; 20 h;
参考文献
Lee, Sunkyung; Yi, Kyu Yang; Kim, Soo-Kyung; Suh, Jeehee; Kim, Nak Jeong; Yoo, Sung-Eun; Lee, Byung Ho; Seo, Ho Won; Kim, Sun-Ok; Lim, Hong
European Journal of Medicinal Chemistry, 2003 , vol. 38, # 5 p. 459 - 471
1: 94.2 percent / Et3N / tetrahydrofuran / 20 °C
2: 96 percent / BH3*THF / tetrahydrofuran / 20 °C
3: 61 percent / NaH / tetrahydrofuran / 0 - 20 °C
4: 87 percent / CF3COOH / CH2Cl2 / 20 h / 20 °C
View Scheme
参考文献
Lee, Sunkyung; Yi, Kyu Yang; Kim, Soo-Kyung; Suh, Jeehee; Kim, Nak Jeong; Yoo, Sung-Eun; Lee, Byung Ho; Seo, Ho Won; Kim, Sun-Ok; Lim, Hong
European Journal of Medicinal Chemistry, 2003 , vol. 38, # 5 p. 459 - 471
1: 96 percent / BH3*THF / tetrahydrofuran / 20 °C
2: 61 percent / NaH / tetrahydrofuran / 0 - 20 °C
3: 87 percent / CF3COOH / CH2Cl2 / 20 h / 20 °C
View Scheme
参考文献
Lee, Sunkyung; Yi, Kyu Yang; Kim, Soo-Kyung; Suh, Jeehee; Kim, Nak Jeong; Yoo, Sung-Eun; Lee, Byung Ho; Seo, Ho Won; Kim, Sun-Ok; Lim, Hong
European Journal of Medicinal Chemistry, 2003 , vol. 38, # 5 p. 459 - 471
1: 61 percent / NaH / tetrahydrofuran / 0 - 20 °C
2: 87 percent / CF3COOH / CH2Cl2 / 20 h / 20 °C
View Scheme
参考文献
Lee, Sunkyung; Yi, Kyu Yang; Kim, Soo-Kyung; Suh, Jeehee; Kim, Nak Jeong; Yoo, Sung-Eun; Lee, Byung Ho; Seo, Ho Won; Kim, Sun-Ok; Lim, Hong
European Journal of Medicinal Chemistry, 2003 , vol. 38, # 5 p. 459 - 471
