(Z)-3,7,11,15-四甲基十六碳-2-烯酸合成路线 （共 2 条）
反应条件
sodium chlorite; sodium dihydrogenphosphate; aminosulfonic acid in water; tert-butyl alcohol
T=20°C; 18 h;
参考文献
Chemgenesis Incorporated
Patent: US2012/264923 A1, 2012 ;
Location in patent: Page/Page column 33 ;
反应条件
1.1: oxalyl dichloride / dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: aminosulfonic acid; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme
参考文献
Chemgenesis Incorporated
Patent: US2012/264923 A1, 2012 ;
