您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
365426-93-3
合成路线
（共 8 条）
626-02-8
3-碘苯酚
+
128796-39-4
4-三氟甲基苯硼酸
→
反应条件
365426-93-3
反应条件
potassium carbonate; palladium 10 on activated carbon in water T=170°C; 0.333333 h; Microwave irradiation;
参考文献
BIOVITRUM AB (publ)
Patent: WO2008/743 A2, 2008 ;
Location in patent: Page/Page column 41 ;
WO 2008/000743 A2
122902-06-1
→
反应条件
365426-93-3
反应条件
2-(N,N-dimethylamino)-pyridine; palladium (II) trifluoroacetate; oxygen; toluene-4-sulfonic acid in dimethyl sulfoxide T=80°C; P=760.051 Torr; 24 h;
参考文献
Izawa, Yusuke; Pun, Doris; Stahl, Shannon S.
Science, 2011 , vol. 333, # 6039 p. 209 - 213
122924-26-9
→
反应条件
365426-93-3
反应条件
hydrogen bromide; oxygen; copper(ll) bromide in 1,4-dioxane; water T=20°C; 20 h; Sealed tube;
参考文献
Kikushima, Kotaro; Nishina, Yuta
RSC Advances, 2013 , vol. 3, # 43 p. 20150 - 20156
108-43-0
3-氯苯酚
+
98-56-6
对氯三氟甲苯
→
反应条件
365426-93-3
反应条件
1: m-monochlorophenol With tetrahydroxydiboron; ethanol; XPhos-Pd-G2; potassium acetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl T=80°C; Miyaura Borylation Reaction; 2 h; Inert atmosphere; 2: 1-chloro-4-(trifluoromethyl)benzene With potassium carbonate in water T=80°C; Suzuki Coupling; 15 h; Inert atmosphere;
参考文献
Molander, Gary A.; Trice, Sarah L. J.; Kennedy, Steven M.
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8678 - 8688
122801-56-3
→
反应条件
365426-93-3
反应条件
hydrogen iodide 2 h; Heating;
参考文献
Mor, Marco; Rivara, Silvia; Lodola, Alessio; Plazzi, Pier Vincenzo; Tarzia, Giorgio; Duranti, Andrea; Tontini, Andrea; Piersanti, Giovanni; Kathuria, Satish; Piomelli, Daniele
Journal of Medicinal Chemistry, 2004 , vol. 47, # 21 p. 4998 - 5008
402-43-7
对溴三氟甲苯
→
反应条件
365426-93-3
反应条件
1: 95 percent / aq. Na2CO3; Pd(PPh3)4 / ethanol; toluene / 2 h / Heating 2: 70 percent / aq. HI / 2 h / Heating View Scheme
参考文献
Mor, Marco; Rivara, Silvia; Lodola, Alessio; Plazzi, Pier Vincenzo; Tarzia, Giorgio; Duranti, Andrea; Tontini, Andrea; Piersanti, Giovanni; Kathuria, Satish; Piomelli, Daniele
Journal of Medicinal Chemistry, 2004 , vol. 47, # 21 p. 4998 - 5008
10365-98-7
3-甲氧基苯硼酸
→
反应条件
365426-93-3
反应条件
1: 95 percent / aq. Na2CO3; Pd(PPh3)4 / ethanol; toluene / 2 h / Heating 2: 70 percent / aq. HI / 2 h / Heating View Scheme
参考文献
Mor, Marco; Rivara, Silvia; Lodola, Alessio; Plazzi, Pier Vincenzo; Tarzia, Giorgio; Duranti, Andrea; Tontini, Andrea; Piersanti, Giovanni; Kathuria, Satish; Piomelli, Daniele
Journal of Medicinal Chemistry, 2004 , vol. 47, # 21 p. 4998 - 5008
128796-39-4
4-三氟甲基苯硼酸
→
反应条件
365426-93-3
反应条件
1: [Pd(CH3CN)4](BF4)2; 6,6'-dimethyl-2,2'-bipyridine; anthraquinone-2-sulfonic acid sodium salt; oxygen / 1-methyl-pyrrolidin-2-one / 4 h / 50 °C / 760.05 Torr 2: dimethyl sulfoxide; 1-methyl-pyrrolidin-2-one / 32 h / 80 °C View Scheme
参考文献
Izawa, Yusuke; Zheng, Changwu; Stahl, Shannon S.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 13 p. 3672 - 3675
Angew. Chem., 2013 , vol. 125, # 13 p. 3760 - 3763,4
