2-(3,5-二甲氧基)-苯基-4,4,5,5-四甲基-(1,3,2)-二噁硼烷合成路线 （共 18 条）
反应条件
bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); 4,4'-di-tert-butyl-2,2'-dipyridyl in tert-butyl methyl ether T=80°C; 1 h; Microwave irradiation; Solvent;
参考文献
Zeqing, Li; Zhibin, Liang; Yuqiang, Wang; Pei, Yu
Research on Chemical Intermediates, 2013 , vol. 39, # 4 p. 1917 - 1926
反应条件
potassium acetate; tris(dibenzylideneacetone)dipalladium (0) in 1,4-dioxane T=110°C; 3 h;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 28 p. 5359 - 5363
反应条件
Cp*Rh(η4-C6Me6) in cyclohexane T=150°C; 32 h;
参考文献
Organic letters, , vol. 3, # 18 p. 2831 - 2833
反应条件
(3,4,7,8-tetramethyl-1,10-phenanthroline)Ir(Bpin)3(cyclooctene); N-ethyl-N,N-diisopropylamine T=80°C; 8 h; GloveboxInert atmosphere; Reagent/catalystSolvent;
参考文献
Preshlock, Sean M.; Ghaffari, Behnaz; Maligres, Peter E.; Krska, Shane W.; Maleczka, Robert E.; Smith, Milton R.
Journal of the American Chemical Society, 2013 , vol. 135, # 20 p. 7572 - 7582
反应条件
IrH(C6H3(NC7H4NC6H2(CH3)3)2)Cl(NCCH3); sodium t-butanolate T=100°C; 24 h; Inert atmosphere;
参考文献
Chianese, Anthony R.; Mo, Allen; Lampland, Nicole L.; Swartz, Raymond L.; Bremer, Paul T.
Organometallics, 2010 , vol. 29, # 13 p. 3019 - 3026
反应条件
1: C14H24BNO2 With methanol in ethyl acetate T=-5 - 20°C; 1 h; Inert atmosphereSchlenk technique; 2: 2,3-dimethylbutane-2,3-diol in diethyl ether T=20°C; 4 h; Inert atmosphereSchlenk technique;
参考文献
Guerrand, Helene D. S.; Marciasini, Ludovic D.; Jousseaume, Melissa; Vaultier, Michel; Pucheault, Mathieu
Chemistry - A European Journal, 2014 , vol. 20, # 19 p. 5573 - 5579
反应条件
1.1: palladium diacetate; potassium iodide; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; triethylamine / ethyl acetate / 16 h / 50 °C / |Inert atmosphere; |Schlenk technique 2.1: methanol / ethyl acetate / 1 h / -5 - 20 °C / |Inert atmosphere; |Schlenk technique 2.2: 4 h / 20 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Chemistry - A European Journal, , vol. 20, # 19 p. 5573 - 5579
反应条件
Oxonereg; in water; acetone T=20°C; 0.5 h;
参考文献
Marshall, Laura J.; Cable, Karl M.; Botting, Nigel P.
Tetrahedron Letters, 2010 , vol. 51, # 20 p. 2690 - 2692
反应条件
copper dichloride in methanol T=90°C;
参考文献
Murphy, Jaclyn M.; Liao, Xuebin; Hartwig, John F.
Journal of the American Chemical Society, 2007 , vol. 129, # 50 p. 15434 - 15435
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium iodide in methanol; water T=80°C; 1 h; High pressure;
参考文献
Partridge, Benjamin M.; Hartwig, John F.
Organic Letters, 2013 , vol. 15, # 1 p. 140 - 143
