3,4-二甲氧基苯硼酸频哪醇酯合成路线 (共 10 条)
反应条件
[2,2']bipyridinyl; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in n-heptane T=25 - 95°C;
参考文献
PIRAMAL ENTERPRISES LIMITED; SIVAKUMAR, Meenakshi; JOSHI, Kalpana, Sanjay; HARIHARAN, Sivaramakrishnan; BOKKA, Ravishankar; AWARE, Valmik, Sopan; MANOHAR, Sonal; SONAWANE, Vinay; CHENNAMSETTY, Suneelmanoharbabu; KALE, Ganesh; THOMAS, Becky, Mary; TRIVEDI, Jacqueline, Vinodkumar
Patent: WO2013/175415 A1, 2013 ;
Location in patent: Page/Page column 46 ;
反应条件
Cp*Rh(η4-C6Me6) in cyclohexane T=150°C; 45 h;
参考文献
Tse; Cho; Smith 3rd.
Organic letters, 2001 , vol. 3, # 18 p. 2831 - 2833
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II); 1,3-bis-(diphenylphosphino)propane; triethylamine in toluene T=100°C; 18 h; Inert atmosphere;
参考文献
Rosen, Brad M.; Huang, Chenghong; Percec, Virgil
Organic Letters, 2008 , vol. 10, # 12 p. 2597 - 2600
反应条件
toluene-4-sulfonic acid in benzene 16 h; Heating;
参考文献
Banwel, Martin G.; Sydnes, Magne O.
Australian Journal of Chemistry, 2004 , vol. 57, # 6 p. 537 - 548
反应条件
iridium(hydrotris(pyrazolyl)borate)(1,5-cyclooctadiene) T=120°C; 16 h;
参考文献
Murata, Miki; Odajima, Hiroki; Watanabe, Shinji; Masuda, Yuzuru
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 12 p. 1980 - 1982
反应条件
in cyclohexane T=100°C; 0.25 h; Inert atmosphere; regioselective reaction;
参考文献
Chemical Communications, , vol. 46, # 41 p. 7724 - 7726
反应条件
1: With bis(dibenzylideneacetone)-palladium(0) in methanol T=20°C; 0.166667 h; Inert atmosphereGlovebox; 2: With potassium fluoride in methanol T=20°C; 24 h; Inert atmosphereGlovebox;
参考文献
Robbins, Daniel W.; Hartwig, John F.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 3 p. 933 - 937
Angew. Chem., 2012 , vol. 125, # 3 p. 967 - 971,5
反应条件
hydrogenchloride; polystyrene boronic acid in acetonitrile T=20°C; 18 h;
参考文献
Pennington, Thomas E.; Kardiman, Cynantya; Hutton, Craig A.
Tetrahedron Letters, 2004 , vol. 45, # 35 p. 6657 - 6660
反应条件
NH4I; Cu(NO3)2*3H2O; oxygen; acetic acid T=130°C; 18 h;
参考文献
Kim, Jinho; Choi, Jiho; Shin, Kwangmin; Chang, Sukbok
Journal of the American Chemical Society, 2012 , vol. 134, # 5 p. 2528 - 2531
反应条件
palladium diacetate; triphenylphosphine; p-benozquinone T=20°C; P=760.051 Torr; 18 h;
参考文献
Yamamoto, Yoshihiko
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 2-3 p. 478 - 492