diethyl ether; sodium amide
und anschliessenden Erwaermen mit Bromaethan oder Diaethylsulfat;
参考文献
Pomerantz et al.
Journal of Research of the National Bureau of Standards (United States), 1954 , vol. 52, p. 59,60
Full Text Show Details
Lewina et al.
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 2195,2198; engl.Ausg.S.2453,2455
n-butyllithium
1.) Et2O, hexane, -80 deg C then r.t., 5 d; 2.) Et2O, hexane, -40 deg C to r.t.; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
n-butyllithium
1.) Et2O, hexane, -80 deg C then r.t., 5 d; 2.) Et2O, hexane, -40 deg C to r.t.; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
Courtneidge, John L.; Davies, Alwyn G.; Lusztyk, Ewa; Lusztyk, Janusz
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 1 p. 155 - 164