in methanol byproducts: AgCl; heated to reflux for 15 min; cooled, filtered, concd., addn. of an aq. soln. of NaClO4, pptn. filtered off, washed with diethyl ether, recrystn. (water or water-methanol 9:1); elem. anal.;
参考文献
Kakoti, Maushumi; Deb, Alok K.; Goswami, Sreebrata
Inorganic Chemistry, 1992 , vol. 31, p. 1302 - 1304
