反应条件
LiCl*H2O in N,N-dimethyl-formamide under N2; RuCl3, bipyridine and LiCl*H2O in DMF stirred and heated at reflux for 8 h; cooled to room temp.; according to S. Rathinasamy et al., J. Enzyme Inhib. Med. Chem., 2006, 21, 501 and Y. Nakabayashi et al., Inorg. Chim. Acta, 2004, 357, 2553; acetone added; maintained at 0°C overnight; centrifuged; ppt. washed with distd. H2O, acetone, EtOH and Et2O;
参考文献
Dalton Transactions, , vol. 40, # 33 p. 8353 - 8360
