in dimethyl sulfoxide suspn. of Pd complex (0.035 mmol), Pd(dba)2 (0.035 mmol), and 2,2'-bipyridine (0.035 mmol) in DMSO stirred at room temp. for 1 d; filtered through Celite, filtrate added to CH2Cl2/Et2O (1/1), ppt. sepd.by centrifugation, dried under vac.; mixt. not sepd.;
参考文献
European Journal of Inorganic Chemistry, , # 9 p. 1394 - 1402
in ethanol EtOH soln. of 2,2-bipyridine added dropwise to EtOH soln. of Pd(MeCN)2Cl2 at 60°C; cooled to room temp. after ca 1 h; filtered; washed with EtOH; dried in vac.;
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 65, # 9 p. 1121 - 1127
