反应条件
1.1: 35percent H2O2; AcOH / 80 °C
2.1: 90percent HNO3; 30percent SO3 / H2SO4 / 110 °C
3.1: AcBr / acetic acid / Heating
4.1: PBr3 / CHCl3
5.1: tetrakis(triphenylphosphine) Pd(0); aq. potassium carbonate / dimethylformamide / 24 h / 85 - 95 °C
5.2: 30.4 percent / dimethylformamide / 5 h / 115 °C
View Scheme
参考文献
Carlson, Brenden; Phelan, Gregory D.; Kaminsky, Werner; Dalton, Larry; Jiang, Xuezhong; Liu, Sen; Jen, Alex K.-Y.
Journal of the American Chemical Society, 2002 , vol. 124, # 47 p. 14162 - 14172