N,N,N',N'-四甲基联苯胺合成路线 (共 97 条)
反应条件
1: With copper dichloride in acetonitrile T=24 - 26°C; 10 h; 2: With potassium carbonate T=24 - 26°C; 0.166667 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 26 p. 9849 - 9852
反应条件
catalyst 1 (aliphatic, phosphine based pincer complex of palladium) in 1,4-dioxane; 1-methyl-pyrrolidin-2-one T=100°C; Negishi cross-coupling reaction; 0.3 h;
参考文献
Dalton Transactions, , vol. 40, # 48 p. 12939 - 12941
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy-KI in tetrahydrofuran; benzene T=63°C; 2.5 h; Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 54, # 20 p. 4844 - 4848
反应条件
1,2-dichloro-ethane; manganese (II) chloride in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Journal of Organometallic Chemistry, , vol. 694, # 5 p. 599 - 603
反应条件
iodic acid; sodium nitrite in water T=20°C; 0.0833333 h; chemoselective reaction;
参考文献
Chemistry Letters, , vol. 39, # 8 p. 808 - 809
反应条件
Me4-DACH; magnesium; cobalt(II) chloride in tetrahydrofuran T=0°C; Inert atmosphere;
参考文献
Synlett, , # 18 p. 2931 - 2934
反应条件
copper dichloride in dimethyl sulfoxide T=80°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 54, # 49 p. 6725 - 6728
反应条件
zirconium tetrachloride; N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide in chloroform 5 h; Reflux;
参考文献
Journal of Fluorine Chemistry, , vol. 154, p. 67 - 72
反应条件
tetra-(n-butyl)ammonium iodide; tetracarbonylbis(μ-chloro)dirhodium(I) in N,N-dimethyl-formamide T=20°C; 24 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, # 11 p. 2364 - 2368
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2580 - 2585