丙-2-基N-(4-甲基苯基)氨基甲酸酯合成路线 (共 7 条)
反应条件
copper diacetate; palladium diacetate; potassium iodide in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=120°C; P=760.051 Torr;
参考文献
Guan, Zheng-Hui; Lei, Hao; Chen, Ming; Ren, Zhi-Hui; Bai, Yinjuan; Wang, Yao-Yu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 489 - 496
参考文献
Baskakow; Mel'nikow
Zhurnal Obshchei Khimii, 1954 , vol. 24, p. 373,377
Chem.Abstr., 1954 , p. 8465
反应条件
Ambient temperature;
参考文献
Vigne; Archelas; Fourneron; Furstoss
Tetrahedron, 1986 , vol. 42, # 9 p. 2451 - 2456
反应条件
1: in tetrahydrofuran
3 h;
2: With water in dichloromethane
参考文献
Ghosh, Rajshekhar; Nethaji, Munirathinam; Samuelson, Ashoka G.
Journal of Organometallic Chemistry, 2005 , vol. 690, # 5 p. 1282 - 1293
反应条件
1: TolSO2N=IPh / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
2: dichloromethane / 4.5 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Yoshimura, Akira; Luedtke, Matthew W.; Zhdankin, Viktor V.
Journal of Organic Chemistry, 2012 , vol. 77, # 4 p. 2087 - 2091
参考文献
Kienzle,F.
Tetrahedron Letters, 1972 , p. 1771 - 1774
反应条件
in toluene
24 h; Heating; Product distribution; Further Variations:Temperatures;
参考文献
Ghosh, Rajshekhar; Samuelson, Ashoka G.
Chemical Communications, 2005 , # 15 p. 2017 - 2019