1: 73 percent / Br2 / acetonitrile / 0.17 h / Heating 2: 55 percent / Br2 / acetonitrile / 1.5 h / Heating 3: 90 percent / NH2OH / ethanol; H2O / 0.25 h / Heating View Scheme

1: 73 percent / Br2 / acetonitrile / 0.17 h / Heating 2: 55 percent / Br2 / acetonitrile / 1.5 h / Heating View Scheme

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '8127930', constants.ctx, '0')">sodium iodide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1099903', constants.ctx, '0')">N,N,N',N',N'',N''-hexamethylphosphoric triamide</a> <br />T=165 - 170&deg;C;&nbsp;<br /> &nbsp;

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<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11342940', constants.ctx, '0')">sodium hydroxide</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3574984', constants.ctx, '0')">N-benzyl-N,N,N-triethylammonium chloride</a> <br /> <br /> &nbsp;