反应条件
1: trifluoroacetic acid / 1 h / 0 °C
2: 77 percent / H2 / RhCl(PPh3)3 / benzene / 24 h
3: 1.) NaIO4, 2.) sodium bicarbonate / 1.) H2O, CH3OH, room temperature, overnight, 2.) toluene, reflux, 16 h
View Scheme
参考文献
Ishibashi, Hiroyuki; Ohnishi, Minako; Senda, Toshihiko; Ikeda, Masazumi
Synthetic Communications, 1989 , vol. 19, # 5and6 p. 857 - 864
