二甲基2-羟基间苯二甲酸酯合成路线 (共 16 条)
反应条件
lithium aluminium tetrahydride
参考文献
Freeman
Journal of the American Chemical Society, 1952 , vol. 74, p. 6257,6258
参考文献
Suh, Junghun; Chun, Keun Ho
Journal of the American Chemical Society, 1986 , vol. 108, # 11 p. 3057 - 3063
反应条件
thionyl chloride in methanol
参考文献
Sankyo Company, Limited
Patent: US6555556 B1, 2003 ;
US 6555556 B1
参考文献
Graebe; Kraft
Chemische Berichte, 1906 , vol. 39, p. 799
反应条件
sodium hydroxide in methanol
T=25°C; pH: 7;
参考文献
Bertz, Steven H.; Dabbagh, Gary
Angewandte Chemie, 1982 , vol. 94, # 4 p. 317 - 318
反应条件
boron tribromide in dichloromethane
T=-78°C; Inert atmosphere;
参考文献
Megens, Rik P.; Van Den Berg, Tieme A.; De Bruijn, A. Dowine; Feringa, Ben L.; Roelfes, Gerard
Chemistry - A European Journal, 2009 , vol. 15, # 7 p. 1723 - 1733
反应条件
sodium hydride in tetrahydrofuran
T=-10°C; 2 h;
参考文献
Covarrubias-Zuniga, Adrian; Rios-Barrios, Eduardo
Journal of Organic Chemistry, 1997 , vol. 62, # 17 p. 5688 - 5689
反应条件
potassium fluoride; acetic acid in 1,4-dioxane
Heating;
参考文献
Takeuchi, Naoki; Okada, Naomi; Tobinaga, Seisho
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4355 - 4359
反应条件
sulfuric acid
24 h; Heating;
参考文献
Suh, Junghun; Chun, Keun Ho
Journal of the American Chemical Society, 1986 , vol. 108, # 11 p. 3057 - 3063
反应条件
triethylamine in tetrahydrofuran
72 h; Heating;
参考文献
Barton, Derek H. R.; Dressaire, Gilles; Willis, Brian J.; Barrett, Anthony G.M.; Pfeffer, Marc
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 665 - 670