potassium methanolate in methanol T=40°C; electrolysis: anode: platinum foil; current source: galvanostat; current density 200 mA cm-2; current consumption: 3.03 F mol-1; cell voltage 50-60 V; Yield given;
参考文献
Weiper-Idelmann, Andreas; Aus Dem Kahmen, Martin; Schaefer, Hans J.; Gockeln, Marianne
Acta Chemica Scandinavica, 1998 , vol. 52, # 6 p. 672 - 682
1: With caesium carbonate in ethanol 2: With Merryfield resin in N,N-dimethyl-formamide T=50°C; 72 h; 3: With di(n-butyl)tin oxide in chlorobenzene T=133°C; 4 h; Further stages. Further byproducts. Title compound not separated from byproducts.;
参考文献
Ruddick, Clare L.; Hodge, Philip; Cook, Anthony; McRiner, Andrew J.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 5 p. 629 - 637
