反应条件
1: AlCl3, aluminium chloride / 1.33 h / 50 °C 2: boric acid trimethyl ester; (S)-(-)-α,α-diphenyl-2-pyrrolidinemethanol; dimethylsulfide borane complex / tetrahydrofuran; toluene / 1.5 h / 35 - 45 °C 3: sodium hydroxide / water; toluene / 1 h / 40 °C 4: sodium t-butanolate / toluene / 11 h / 60 - 80 °C View Scheme
参考文献
Zhang, Hao; Liu, Jun; Zhang, Luyong; Kong, Lingyi; Yao, Hequan; Sun, Hongbin
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 11 p. 3598 - 3602