1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; Inert atmosphere; 2: in tetrahydrofuran; hexane T=-78 - 20°C; Inert atmosphere; 3: With hydrogenchloride; water in tetrahydrofuran; hexane Inert atmosphere;
参考文献
Chen, Wei-Hong; Chuang, Wei-Tsung; Jeng, U-Ser; Sheu, Hwo-Shuenn; Lin, Hong-Cheu
Journal of the American Chemical Society, 2011 , vol. 133, # 39 p. 15674 - 15685