反应条件
1.1: n-butyllithium; N,N,N',N'-tetramethylethylenediamine / tetrahydrofuran
1.2: 95 percent / 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / tetrahydrofuran
2.1: n-butyllithium; N,N,N',N'-tetramethylethylenediamine / tetrahydrofuran; hexane / 1 h / -78 °C
2.2: trimethyl borate / tetrahydrofuran; hexane / 1.5 h / -78 °C
2.3: 61 percent / aq. HCl / tetrahydrofuran; hexane / 20 °C
View Scheme
参考文献
Deeg, Oliver; Baeurle, Peter
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 9 p. 1609 - 1624
