1: bromine; trifluoroacetic acid / 20 °C 2: potassium carbonate / acetonitrile / 15 h / 20 °C View Scheme
参考文献
Givens, Richard S.; Stensrud, Kenneth; Conrad, Peter G.; Yousef, Abraham L.; Perera, Chamani; Senadheera, Sanjeewa N.; Heger, Dominik; Wirz, Jakob
Canadian Journal of Chemistry, 2011 , vol. 89, # 3 p. 364 - 384
Baker; Kaeding
Journal of the American Chemical Society, 1959 , vol. 81, p. 5904,5905
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Klaassens; Schoot
Recueil des Travaux Chimiques des Pays-Bas, 1956 , vol. 75, p. 186
1: sodium hydride / ethylene glycol dimethyl ether; mineral oil / 15 h / 23 °C / Inert atmosphere 2: sodium t-butanolate / bis(1,5-cyclooctadiene)nickel (0); SIDip*HCl / 1,4-dioxane / 3 h / 80 °C / Inert atmosphere 3: trifluoroacetic acid; N-iodo-succinimide / 14 h / 23 °C / Inert atmosphere; Sealed vessel 4: potassium carbonate / trans-1,2-cyclohexanediamine; copper(l) chloride / 1,4-dioxane / 15 h / 110 °C / Inert atmosphere; Darkness; Sealed vessel 5: 7 h / 23 °C / Inert atmosphere View Scheme
参考文献
THE REGENTS OF THE UNIVERSITY OF CALIFORNIA; GARG, Neil K.; RAMGREN, Stephen D.; SILBERSTEIN, Amanda L.; QUASDORF, Kyle W.
Patent: WO2012/94622 A2, 2012 ;
