反应条件
1: 44 percent / NaOH / ethanol; H2O / 0.5 h / 65 - 70 °C 2: 1.) SnCl4, 2.) conc. HCl / 1.) CH2Cl2, RT, 30 min., 2.) H2O, CH2Cl2, 1.5 h 3: 88.5 percent / NH4OAc / 4 h / Heating 4: LiAlH4 / tetrahydrofuran; diethyl ether / 1.5 h / Ambient temperature View Scheme
参考文献
Glennon; Young; Benington; Morin
Journal of Medicinal Chemistry, 1982 , vol. 25, # 10 p. 1163 - 1168
