ammonia in tetrahydrofuran T=20°C; 0.5 h;

hydrogenchloride

1: Acetylieren und anschliessend Nitrieren 2: aqueous HCl View Scheme

1: HNO3+H2SO4 2: alcohol; ammonia View Scheme

暂无反应条件数据

1: potassium hydroxide / tetrahydrofuran; water / 0.5 h / 20 °C 2: sodium hydrogensulfide / tetrahydrofuran / 3 h / Reflux View Scheme

hydrogenchloride; tin 2 h; Heating;

hydrogenchloride; tin 2 h; Heatingother reaction route; Product distribution;

1.1: conc. sulfuric acid; aq. sodium nitrite / acetic acid / 0 °C 1.2: aq. sodium azide / 1 h / 20 °C 2.1: 810 mg / ethyl acetate / 2.5 h / Heating 3.1: 52 percent / triphenylphosphine / ethyl acetate / 1 h / Heating 4.1: 4.7 percent / conc. hydrochloric acid; iron powder / CH2Cl2; methanol / 0.25 h / 20 °C View Scheme

1: With sulfuric acid; sodium nitrite in acetic acid T=0°C; 2: With sodium azide T=20°C; 1 h;