Anderson, David D.; Beutel, Bruce A.; Cooper, Curt S.; Gu, Yu-Gui; Hinman, Mira M.; Kalvin, Douglas M.; Keyes, Robert F.; Searle, Xenia B.; Wagner, Rolf
Patent: US2005/159423 A1, 2005 ;
Location in patent: Page/Page column 20 ;
1.1: 16 h / 110 - 115 °C
2.1: dowtherm A / 2 h / 240 - 245 °C
2.2: 2 h / 110 °C
3.1: 2.5 h / 185 - 195 °C / 6 - 7.5 Torr
4.1: Raney Ni / ethanol / Reflux
4.2: 16 h
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