(S)-(-)-N-(三氟乙酰基)吡咯烷-2-羰酰氯合成路线 （共 3 条）
反应条件
pyridine; oxalyl dichloride in benzene 1 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 52, # 8 p. 1627 - 1630
反应条件
1: 73 percent / KOMe / methanol / 40 °C 2: Vilsmeier reagent / various solvent(s) / 3 h / -12 - -10 °C View Scheme
参考文献
Tetrahedron, , vol. 59, # 45 p. 9019 - 9029
反应条件
1: 85 percent / AlCl3 / CH2Cl2 / 12 h / Ambient temperature
2: 85 percent / H2 / Pd/C / ethanol; diethyl ether
3: 65 percent / K2CO3 / methanol; H2O
View Scheme
参考文献
Nordlander, J. Eric; Njoroge, F. George; Payne, Mark J.; Warman, Dhiraj
Journal of Organic Chemistry, 1985 , vol. 50, # 19 p. 3481 - 3484
