4-(4-氨基苯基)-2-氨基噻唑合成路线 （共 5 条）
反应条件
iodine T=130 - 150°C; 0.166667 h; Neat (no solvent)Microwave irradiation;
参考文献
Caceres-Castillo, David; Carballo, Ruben M.; Tzec-Interian, Jorge A.; Mena-Rejon, Gonzalo J.
Tetrahedron Letters, 2012 , vol. 53, # 30 p. 3934 - 3936
反应条件
thiourea in DMF on palladium; carbon
参考文献
Boehringer Ingelheim Pharma KG
Patent: US6043254 A1, 2000 ;
US 6043254 A
反应条件
iron; ammonium chloride in water; isopropyl alcohol 1 h; Reflux;
参考文献
FUJIFILM Corporation; TATEISHI, Keiichi; FUJIE, Yoshihiko; TANAKA, Shigeaki
Patent: EP2604656 A1, 2013 ;
Location in patent: Paragraph 0298; 0300 ;
反应条件
1.1: water / 5 h / 70 °C 1.2: 3 h / 20 °C 2.1: iron; ammonium chloride / water; isopropyl alcohol / 1 h / |Reflux View Scheme
反应条件
iron; ammonium chloride in acetone T=4°C; 0.25 h;
参考文献
FUJIFILM Corporation; TATEISHI, Keiichi; FUJIE, Yoshihiko; TANAKA, Shigeaki
Patent: EP2604656 A1, 2013 ;
Location in patent: Paragraph 0317; 0319 ;
