甲基2,3-二溴-2-甲基丙酸酯合成路线 （共 15 条）
反应条件
N1-methyl-N1-phenyl hydrazine; triethylamine in acetonitrile
1.)25 deg C, 1 month 2.)reflux, 18 h;
参考文献
Prosyanik, A. V.; Markov, V. I.; Bondarenko, S. V.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2171 - 2174
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 12 p. 2480 - 2484
反应条件
sodium hydride in N,N-dimethyl-formamide
T=120°C; 8 h;
参考文献
Salimbeni; Manghisi
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 3 p. 489 - 492
反应条件
1: 92 percent / methanol / 1 h / Heating
2: aq. HCl / 1 h / 20 °C
View Scheme
参考文献
Gambacorta, Augusto; Farah, Mohamed Elmi; Tofani, Daniela
Tetrahedron, 1999 , vol. 55, # 43 p. 12615 - 12628
反应条件
1: in acetonitrile
12 h; Heating;
2: With water in acetonitrile
T=20°C; Further stages.;
参考文献
Khachikyan; Tovmasyan; Indzhikyan
Russian Journal of General Chemistry, 2007 , vol. 77, # 6 p. 1034 - 1036
反应条件
1: in acetonitrile
T=20°C; 0.25 h;
2: With water in acetonitrile
T=20°C; Further stages.;
参考文献
Khachikyan; Tovmasyan; Indzhikyan
Russian Journal of General Chemistry, 2007 , vol. 77, # 6 p. 1034 - 1036
