反应条件
1: 1.) conc. H2SO4, (CH3)2CH2CH2CH2ONO, 2.) 26percent aq. Me2NH, Na2CO3 / 1.) DMF, -10 deg C, 30 min, 2.) DMF, H2O, 20 deg C, 1 h
2: 60 percent / H2 / 10percent Pd/C / ethanol / 15 h / 1551.4 Torr / Ambient temperature
View Scheme
参考文献
Brown, Roger F. C.; Coulston, Karen J.; Eastwood, Frank W.; Jurss, Craig J.
Australian Journal of Chemistry, 1994 , vol. 47, # 3 p. 566 - 570
