反式,反式-法尼基酸甲酯合成路线 (共 42 条)
反应条件
n-butyllithium
1) THF-hexan, -78 deg C, 1.5 h, 2) -78 deg C, 1 h, room temperature, 15 h; Yield given. Multistep reaction;
参考文献
Odinokov, V. N.; Kukovinets, O. S.; Sakharova, N. I.; Tolstikov, G. A.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 6 p. 1075 - 1077
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 6 p. 1180 - 1182
参考文献
Tatarazako, Norihisa; Oda, Shigeto; Watanabe, Hajime; Morita, Masatoshi; Iguchi, Taisen
Chemosphere, 2003 , vol. 53, # 8 p. 827 - 833
反应条件
1: (i) NaH, Et2O, (ii) /BRN= 471433/
2: (i) CuI, Et2O, (ii) /BRN= 5116697/
View Scheme
参考文献
Sum,F.-W.; Weiler,L.
Canadian Journal of Chemistry, 1979 , vol. 57, p. 1431 - 1441
反应条件
(i) , (ii) aq. H2SO4; Multistep reaction;
参考文献
Burrell,J.W.K. et al.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 2144 - 2154
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Savu, Patricia M.; Katzenellenbogen, John A.
Journal of Organic Chemistry, 1981 , vol. 46, # 2 p. 239 - 250
反应条件
(i), (ii) /BRN= 605437/, (iii) PhSH, (iv) /BRN= 1209226/, CuI; Multistep reaction;
参考文献
Kobayashi,S.; Mukaiyama,T.
Chemistry Letters, 1974 , p. 1425 - 1428
参考文献
Kobayashi,S. et al.
Chemistry Letters, 1977 , p. 1169 - 1172
反应条件
N-bromosuccinmide in tetrahydrofuran; water
1) 0 deg C, 1.5h, 2) 20 deg C, 1 h;
参考文献
Odinokov, V. N.; Kukovinets, O. S.; Sakharova, N. I.; Tolstikov, G. A.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 6 p. 1075 - 1077
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 6 p. 1180 - 1182
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=-20°C;
参考文献
Camps, F.; Messeguer, A.; Sanchez, Francisco-Jose
Tetrahedron, 1988 , vol. 44, # 16 p. 5161 - 5168
反应条件
cholic acid-Na-salt; linoleic acid hydroperoxide; phosphat buffer
72 h; Ambient temperature; Mechanism;
参考文献
Meyer, Werner; Spiteller, Gerhard
Liebigs Annalen der Chemie, 1993 , # 12 p. 1253 - 1256