4-(三氟甲基)苯甲酰氟合成路线 （共 10 条）
反应条件
CsSO4F in acetonitrile T=30 - 35°C; 1 h;
参考文献
Stavber, Stojan; Kosir, Iztok; Zupan, Marko
Journal of Organic Chemistry, 1997 , vol. 62, # 15 p. 4916 - 4920
反应条件
CsSO4F in acetonitrile T=35°C; 1.5 h;
参考文献
Stavber, Stojan; Planinsek, Zdenka; Zupan, Marko
Journal of Organic Chemistry, 1992 , vol. 57, # 20 p. 5334 - 5337
反应条件
sulfur(IV) fluoride T=120°C; unter Druck;
参考文献
Hasek,W.R. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 543 - 551
Full Text View citing articles Show Details
Du Pont de Nemours and Co.
Patent: US2859245 , 1956 ;
反应条件
sulfur(IV) fluoride; boron trifluoride T=130°C; 8 h;
参考文献
Hasek,W.R. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 543 - 551
反应条件
potassium fluoride; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=80°C; Inert atmosphereSealed tube;
参考文献
Ueda, Tsuyoshi; Konishi, Hideyuki; Manabe, Kei
Organic Letters, 2013 , vol. 15, # 20 p. 5370 - 5373
反应条件
fluorine in acetonitrile T=0°C; Inert atmosphere;
参考文献
Chambers, Richard D.; Sandford, Graham; Trmcic, Jelena; Okazoe, Takashi
Organic Process Research and Development, 2008 , vol. 12, # 2 p. 339 - 344
反应条件
potassium hydrogen difluoride; 18-crown-6 ether
参考文献
Laclef, Sylvain; Exner, Claudia J.; Turks, Maris; Videtta, Valeria; Vogel, Pierre
Journal of Organic Chemistry, 2009 , vol. 74, # 22 p. 8882 - 8885
参考文献
Gen. Aniline Works
Patent: US2181554 , 1937 ;
Full Text Show Details
I.G. Farbenind.
Patent: DE707955 , 1936 ;
DRP/DRBP Org.Chem.
参考文献
Brownlee, Robert T. C.; Craik, David J.
Organic Magnetic Resonance, 1980 , vol. 14, # 3 p. 186 - 191
参考文献
I.G. Farbenind.
Patent: DE707955 , 1936 ;
DRP/DRBP Org.Chem.
