3-异硫氰酸吡啶甲酯氢溴酸合成路线 （共 5 条）
反应条件
hydrazine in ethanol Yield given;
参考文献
Rahman, M. F.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 9 p. 828 - 830
反应条件
in dichloromethane
T=20°C; 24 h;
参考文献
Rajski, Scott R.; Mays, Jared Rae
Patent: US2013/116203 A1, 2013 ;
Location in patent: Paragraph 0095; 0103 ;
反应条件
1: NEt3 / dioxane / 0 deg C to r.t.
2: dioxane / 0 °C
3: NEt3 / dioxane; CHCl3 / Ambient temperature
View Scheme
参考文献
Hirashima, Akinori; Yoshii, Yutaka; Eto, Morifusa
Bioscience, Biotechnology, and Biochemistry, 1992 , vol. 56, # 7 p. 1062 - 1065
反应条件
1: dioxane / 0 °C
2: NEt3 / dioxane; CHCl3 / Ambient temperature
View Scheme
参考文献
Hirashima, Akinori; Yoshii, Yutaka; Eto, Morifusa
Bioscience, Biotechnology, and Biochemistry, 1992 , vol. 56, # 7 p. 1062 - 1065
反应条件
1: hydrazine / ethanol
2: ethanol / 0.5 h / Ambient temperature
View Scheme
参考文献
Rahman, M. F.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 9 p. 828 - 830
