2-(4-甲氧基苯基)-2H-吲唑合成路线 (共 17 条)
反应条件
copper(l) iodide; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran
Molecular sieveInert atmosphere;
参考文献
Hu, Jiantao; Cheng, Yongfeng; Yang, Yiqing; Rao, Yu
Chemical Communications, 2011 , vol. 47, # 36 p. 10133 - 10135
反应条件
1: acetic acid / methanol / 20 °C / Inert atmosphere
2: copper(l) iodide; N,N,N',N,-tetramethylethylenediamine / tetrahydrofuran / Molecular sieve; Inert atmosphere
View Scheme
参考文献
Hu, Jiantao; Cheng, Yongfeng; Yang, Yiqing; Rao, Yu
Chemical Communications, 2011 , vol. 47, # 36 p. 10133 - 10135
反应条件
1: 90 percent / 0.03 h / microwave irradiation
2: 82 percent / triethyl phosphite / 0.07 h / 70 - 150 °C / microwave irradiation
View Scheme
参考文献
Varughese, Deepu John; Manhas, Maghar S.; Bose, Ajay K.
Tetrahedron Letters, 2006 , vol. 47, # 38 p. 6795 - 6797
反应条件
1: isopropyl alcohol / 0.17 h / |Reflux
2: triphenylphosphine; MoO2Cl2(dmf)2 / toluene / 0.17 h / 150 °C / 15001.5 Torr / |Microwave irradiation
View Scheme
参考文献
Moustafa, Ahmed H.; Malakar, Chandi C.; Aljaar, Nayyef; Merisor, Elena; Conrad, Juergen; Beifuss, Uwe
Synlett, 2013 , vol. 24, # 12 art. no. ST-2013-D0283-L, p. 1573 - 1577
反应条件
1: alcohol
2: zinc dust; glacial acetic acid
View Scheme
参考文献
Busch; Hartmann
Journal fuer Praktische Chemie (Leipzig), 1895 , vol. <2>52, p. 405
参考文献
Busch; Hartmann
Journal fuer Praktische Chemie (Leipzig), 1895 , vol. <2>52, p. 405
反应条件
Yield given. Multistep reaction;
参考文献
Frontana-Uribe, Bernardo A.; Moinet, Claude
Tetrahedron, 1998 , vol. 54, # 13 p. 3197 - 3206