4-(2-甲氧基乙氧基)-苯甲醛合成路线 （共 7 条）
反应条件
sodium hydroxide in dichloromethane; water
Substitution; Williamson reaction; 16 h;
参考文献
Sebhat, Iyassu K.; Tan, Yen-Ling; Widdowson, David A.; Wilhelm, Rene; White, Andrew J.P.; Williams, David J.
Tetrahedron, 2000 , vol. 56, # 33 p. 6121 - 6134
反应条件
potassium carbonate in dimethyl sulfoxide
T=20°C; 72 h;
参考文献
FMC CORPORATION
Patent: WO2005/36961 A2, 2005 ;
Location in patent: Page/Page column 54-55 ;
反应条件
sodium methylate in methanol; 1-chloro-2-methoxy-ethane
参考文献
Giffels, Guido; Dreisbach, Claus
Patent: US2001/14697 A1, 2001 ;
反应条件
potassium carbonate in methanol
T=100°C; 0.25 h; microwave irradiation;
参考文献
Sarju, Julien; Danks, Timothy N.; Wagner, Gabriele
Tetrahedron Letters, 2004 , vol. 45, # 41 p. 7675 - 7677
反应条件
in N,N-dimethyl-formamide
参考文献
Board of Regents of the University of Oklahoma
Patent: US5098903 A1, 1992 ;
反应条件
1: With p-toluenesulfonyl chloride; sodium hydroxide
T=0°C; 5 h;
2: With potassium carbonate in tetrahydrofuran
16 h; Reflux;
参考文献
Yi, Wei; Cao, Rihui; Chen, Zhiyong; Yu, Liang; Wen, Huan; Yan, Qin; Ma, Lin; Song, Huacan
Chemical and Pharmaceutical Bulletin, 2010 , vol. 58, # 5 p. 752 - 754
反应条件
ethanol
T=160 - 170°C;
参考文献
Weygand; Gabler; Bircan
Journal fuer Praktische Chemie (Leipzig), 1941 , vol. <2>158, p. 266,272
