4-亚甲基四氢-2H-吡喃合成路线 （共 26 条）
反应条件
sodium hydroxide; benzenesulfonic Acid
参考文献
BASF Aktiengesellschaft
Patent: US5001242 A1, 1991 ;
反应条件
in diethyl ether
T=25°C; 0.5 h;
参考文献
Margot, Christian; Rizzolio, Michele; Schlosser, Manfred
Tetrahedron, 1990 , vol. 46, # 7 p. 2411 - 2424
反应条件
potassium hydrogensulfate
T=140 - 150°C; 1 h; distillation;
参考文献
Booth, Harold; Kheidhair, Kheidhair A.; Readshaw, Simon A.
Tetrahedron, 1987 , vol. 43, # 20 p. 4699 - 4724
反应条件
1: 1.) Mg / 1.) ether 2.) ether, 16 h
2: potassium hydrogen sulphate / 1 h / 140 - 150 °C / distillation
View Scheme
参考文献
Booth, Harold; Kheidhair, Kheidhair A.; Readshaw, Simon A.
Tetrahedron, 1987 , vol. 43, # 20 p. 4699 - 4724
反应条件
potassium hydrogensulfate
参考文献
Du Pont de Nemours and Co.
Patent: US2789996 , 1953 ;
反应条件
1: 200 °C
2: potassium hydrogen sulfate
View Scheme
参考文献
Du Pont de Nemours and Co.
Patent: US2789996 , 1953 ;
反应条件
sulfuric acid
T=40 - 80°C; Kinetics;
参考文献
Ryvkina; Sinitsyn
Russian Journal of Applied Chemistry, 1998 , vol. 71, # 8 p. 1479 - 1481
反应条件
hydrogen; palladium
T=120 - 180°C; other catalysts, other temperatures; Product distribution;
参考文献
Ibatullin, U. G.; Mukhanetova, D. Ya.; Vasil'eva, S. A.; Talipov, R. F.; Syurina, L. V.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, p. 1866 - 1873
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 9 p. 2114 - 2121
反应条件
sodium hydroxide; pentacarbonyliron(0)
T=180°C; 10 h; autoclave, other time; Product distribution;
参考文献
Ibatullin, U. G.; Petrushina, T. F.; Akhmadeeva, A. A.; Safarov, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 3 p. 262 - 264
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , vol. 21, # 3 p. 318 - 320
参考文献
Ibatullin, U. G.; Talipov, R. F.; Al'mukhametov, E. A.; Safarov, M. G.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 1 p. 87 - 91
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 1 p. 101 - 106
