1-(2-苯并噻唑)-2-丙酮合成路线 （共 16 条）
反应条件
sodium tetrahydroborate in methanol; diethyl ether T=0°C; 0.5 h; Yield given;
参考文献
Fogagnolo, Marco; Giovannini, Pier Paolo; Guerrini, Alessandra; Medici, Alessandro; Pedrini, Paola; Colombi, Nicola
Tetrahedron Asymmetry, 1998 , vol. 9, # 13 p. 2317 - 2327
反应条件
hydrogenchloride anschliessend mit wss. NaOH behandeln;
参考文献
Journal of the Chemical Society, , p. 1619
反应条件
perchloric acid in acetic acid
参考文献
Hoechst Aktiengesellschaft
Patent: US4727154 A1, 1988 ;
反应条件
potassium ethanolate; benzene
参考文献
Stepanow; Dawydowa
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 891,894; engl. Ausg. S. 864, 866
反应条件
in diethyl ether
1) -78 deg C, 1 h, 2) to 0 deg C;
参考文献
Costa, Maria Virginia; Brembilla, Alain; Roizard, Denis; Lochon, Pierre
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 6 p. 1541 - 1544
反应条件
1: phenyllithium / benzene; diethyl ether / -78 °C
2: 50 percent / diethyl ether / 1) -78 deg C, 1 h, 2) to 0 deg C
View Scheme
参考文献
Costa, Maria Virginia; Brembilla, Alain; Roizard, Denis; Lochon, Pierre
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 6 p. 1541 - 1544
反应条件
in tetrahydrofuran
T=65 - 70°C; 3 h; argon atmosphere;
参考文献
Ostroumov, I. G.; Tsil'ko, A. E.; Maretina, I. A.; Petrov, A. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 6 p. 1049 - 1055
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 6 p. 1165 - 1172
反应条件
in tetrahydrofuran
T=65 - 70°C; 3 h; argon atmosphere;
参考文献
Ostroumov, I. G.; Tsil'ko, A. E.; Maretina, I. A.; Petrov, A. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 6 p. 1049 - 1055
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 6 p. 1165 - 1172
反应条件
in tetrahydrofuran
T=65 - 70°C; 3 h; argon atmosphere;
参考文献
Ostroumov, I. G.; Tsil'ko, A. E.; Maretina, I. A.; Petrov, A. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 6 p. 1049 - 1055
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 6 p. 1165 - 1172
参考文献
Ried; Marx
Chemische Berichte, 1957 , vol. 90, p. 2683,2686
Full Text Show Details
Du Pont de Nemours and Co.
Patent: US2323504 , 1939 ;
Full Text Show Details
Stepanow; Dawydowa
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 891,894; engl. Ausg. S. 864, 866
