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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
苯戊醛
合成路线
（共 41 条）
167693-07-4
4,4,5,5-四甲基-2- (4-苯基丁基)-1,3,2-二噁硼烷
→
反应条件
36884-28-3
苯戊醛
反应条件
1: With n-butyllithium; zinc(II) chloride in tetrahydrofuran; hexane; dichloromethane 2: With sodium hydroxide; NaBO3 in tetrahydrofuran T=20°C;
参考文献
Lebel, Helene; Ladjel, Chehla
Journal of Organometallic Chemistry, 2005 , vol. 690, # 23 p. 5198 - 5205
10521-91-2
苯戊醇
+
6729-60-8
三邻甲苯基二氯化铋
→
反应条件
36884-28-3
苯戊醛
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in toluene T=20°C; 2 h;
参考文献
Matano, Yoshihiro; Nomura, Hazumi
Angewandte Chemie - International Edition, 2002 , vol. 41, # 16 p. 3028 - 3031
28525-69-1
5-苯基-4-戊烯酸
→
反应条件
36884-28-3
苯戊醛
反应条件
1: thionyl chloride / 1.5 h / Heating 2: K2CO3 / benzene; diethyl ether / Ambient temperature 3: lithium aluminum hydride (LAH) 4: 15 percent / acetonitrile / Irradiation View Scheme
参考文献
Lewis, Frederick D.; Dasharatha Reddy; Schneider, Siegfried; Ga, Michael
Journal of the American Chemical Society, 1991 , vol. 113, # 9 p. 3498 - 3506
131529-92-5
→
反应条件
36884-28-3
苯戊醛
反应条件
1: lithium aluminum hydride (LAH) 2: 15 percent / acetonitrile / Irradiation View Scheme
参考文献
Lewis, Frederick D.; Dasharatha Reddy; Schneider, Siegfried; Ga, Michael
Journal of the American Chemical Society, 1991 , vol. 113, # 9 p. 3498 - 3506
201230-82-2
+
768-56-9
4-苯基-1-丁烯
→
反应条件
36884-28-3
苯戊醛
反应条件
1: 1-buten-4-yl-benzene With Rh(CO)2(acac); 6-DPPon in tetrahydrofuran T=20°C; Inert atmosphere; 2: carbon monoxide With hydrogen in tetrahydrofuran T=20°C; 20 h; Ambient pressure; regioselective reaction;
参考文献
Kemme, Susanne T.; Smejkal, Tomas; Breita, Bernhard
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 7-8 p. 989 - 994
21087-29-6
肉桂基氯
→
反应条件
36884-28-3
苯戊醛
反应条件
1: 75 percent 2: 75 percent / NaCl / dimethylsulfoxide; H2O / 6 h / Heating 3: 10percent KOH / methanol; H2O / 2 h / Heating 4: thionyl chloride / 1.5 h / Heating 5: K2CO3 / benzene; diethyl ether / Ambient temperature 6: lithium aluminum hydride (LAH) 7: 15 percent / acetonitrile / Irradiation View Scheme
参考文献
Lewis, Frederick D.; Dasharatha Reddy; Schneider, Siegfried; Ga, Michael
Journal of the American Chemical Society, 1991 , vol. 113, # 9 p. 3498 - 3506
22768-07-6
→
反应条件
36884-28-3
苯戊醛
反应条件
1: 10percent KOH / methanol; H2O / 2 h / Heating 2: thionyl chloride / 1.5 h / Heating 3: K2CO3 / benzene; diethyl ether / Ambient temperature 4: lithium aluminum hydride (LAH) 5: 15 percent / acetonitrile / Irradiation View Scheme
参考文献
Lewis, Frederick D.; Dasharatha Reddy; Schneider, Siegfried; Ga, Michael
Journal of the American Chemical Society, 1991 , vol. 113, # 9 p. 3498 - 3506
79685-62-4
→
反应条件
36884-28-3
苯戊醛
反应条件
1: K2CO3 / benzene; diethyl ether / Ambient temperature 2: lithium aluminum hydride (LAH) 3: 15 percent / acetonitrile / Irradiation View Scheme
参考文献
Lewis, Frederick D.; Dasharatha Reddy; Schneider, Siegfried; Ga, Michael
Journal of the American Chemical Society, 1991 , vol. 113, # 9 p. 3498 - 3506
1242310-05-9
→
反应条件
反应条件
Mukaiyama's reagent; O-TMS quinidine; N-ethyl-N,N-diisopropylamine in dichloromethane T=23°C; 24 h; Inert atmosphere; optical yield given as percent dediastereoselective reaction;
参考文献
Morris, Kay A.; Arendt, Kevin M.; Oh, Seong Ho; Romo, Daniel
Organic Letters, 2010 , vol. 12, # 17 p. 3764 - 3767
19710-56-6
+
768-56-9
4-苯基-1-丁烯
→
反应条件
40654-82-8
+
36884-28-3
苯戊醛
反应条件
dicarbonylacetylacetonato rhodium (I); hydrogen; (Me)CgPPh in toluene T=80°C; P=15001.5 Torr; 2 h;
参考文献
Noonan, Gary M.; Fuentes, Jose A.; Cobley, Christopher J.; Clarke, Matthew L.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 10 p. 2477 - 2480
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